[CEPT] Solvothermal synthesis nano zinc oxide in microwave reactor MSS2
|Jacek Wojnarowicz , Tadeusz Chudoba , Witold Łojkowski , Sylwia Kuśnieruk , Elżbieta Pietrzykowska , Aleksandra Kędzierska , Agnieszka Opalińska|
Polish Academy of Sciences, Institute of High Pressure Physics (UNIPRESS), Sokolowska 29/37, Warszawa 01-142, Poland
(CH3CO2) 2Zn → ZnO
Synthesis of nano-zinc oxide doped with cobalt take place in solution of ethylene glycol during 12 minutes in microwave reactor MSS2. Specific surface doped ZnO is 10-50 m2/g and crystallites size are in a range from 20 to 150 nm.
Microwave, pressure chemical reactor MSS2 is used to carry out solvo- and hydrothermal microwavesynthesis, wherein is obtained nanopowders with specific particle size and morphology. Used solutions in the reactor overtake a global level and allows to obtain ultrapure nanoparticles in the production and experimental scale. Developed high-pressure seals provide insert of substrates, running processes, released products in track made from chemically inert materials.
Presentation: Poster at Nano and Advanced Materials Workshop and Fair, by Jacek Wojnarowicz
See On-line Journal of Nano and Advanced Materials Workshop and Fair
Submitted: 2013-09-10 09:49 Revised: 2013-09-10 10:22
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