It will be presented for the first time the new route of chemical synthesis of lithium metal phosphates - LiMPO₄ (where M = Fe, Mn, Co, Ni) of olivine structure. All materials have higher working potential (4 - 5 V vs. Li/Li⁺) than commercially used lithium cobalt (LiCoO₂) or nickel oxides (LiNiO₂) as a positive electrode in lithium-ion batteries. The olivine structure (crystallize in the orthorombic space group Pnma) is stable than structure which represents the layered oxides, due to strong covalent bonds between oxygen ions and P⁵⁺ resulting in PO₄^3- tetrahedral polyanions. The so-obtained powders were characterized by several complementary methods, including structural, morphological and electrochemical studies.

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