The lecture is focused on fundamentals and mechanisms of processes for producing thin-layered materials by the electroless and electrocrystalization methods. Features of various techniques and technologies with using these methods are presented. Possibilities of forming such different structures as: amorphous, nanocrystalline, microcrystalline as well as composite are exhibited. Influences of the process parameters on the material structures and properties are described. Identification of morphologies of the thin-layered materials by using SEM, AFM, RTG, TEM techniques as well optic microscopy are presented. Examples of various structures of materials

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1. Raman spectroscopy studies of metal - carbon nanotubes composite materials.
2. Characterization of nanocrystalline Ni surface layers electrodeposited in Watts bath with additions of ionic liquids
3. The structure and properties of Ni-P/CNTs composite layers produced by chemical method
4. Characterization of Ni-P surface layers produced by the chemical method in a multicomponent solvent with additions of ionic liquids
5. Nanocrystalline nickel surface layers produced electrochemically and their corrosion resistance
6. Electrolytic composite nickel layers with nano-sized Si₃N₄ disperse phase
7. Preparation and characterization of nanocrystalline copper layers
8. Microstructure of Ni-P thin layers obtained by a chemical method