The new Incoatec Microfocus Source IμS™ with molybdenum anode, a 30 W air cooled sealad tube microfocus X-ray source, with a new type of 2-dim beam shaping Montel optics, the so called Quazar™ optics, was mounted at a mar desktop beamline equipped with mar345 imaging plate detector (figure 1). This setup was used to investigate phase transitions of different samples under high pressure and high temperature. For this purpose a diamond anvil cell or a heater was mounted on the goniometer respectively.

To process the data precise information about the sample to detector distance and the detector orientation is necessary. To receive this information, measurements of the standard LaB₆ were done under the same conditions as the measurements of the samples. The data were processed using the program package Powder3D (Dinnebier et al.) for integration and visualisation.
Figure 1: IμS™ for 2-dim diffraction, combined with a mar desktop beamline and mar345 imaging plate detector

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1. Microfocus solutions for X-ray diffractometry with area detectors
2. The Incoatec Microfocus Source IμS™ for home-lab diffractometry
3. Powder diffraction on a Pilatus 100K pixel detector
4. Kinetics of phase transformations of copper phthalocyanine pigments
5. The high pressure crystal structure of the NLO compound BiB₃O₆ from 2D powder diffraction data
6. Parametric refinement of in-situ XRPD data