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Effects of calcination on the electrophoretic deposition of chemically synthesized and naturally derived hydroxyapatite

Onder Albayrak 1Cinar Oncel 2Mustafa Tefek 3Sabri Altintas 1

1. Bogazici University, Istanbul 34342, Turkey
2. Sabanci University, Istanbul 34956, Turkey
3. Mersin University, Mersin 33343, Turkey

Abstract

In this study, electrophoretic deposition (EPD) method was used for hydroxyapatite (HA) coating on titanium substrates. Chemically synthesized nanopowders and naturally derived submicron powders of HA were produced and used as coating materials before and after calcination. Obtained coatings were sintered at 1000 °C for 1 hour. Besides HA coating, two applications including TiO2 were performed: HA/TiO2 composite coating in the one hand, and TiO2 inner coating layer between titanium substrate and HA coating in the other. Results showed that, plate-like shaped nanosized HA powders with aspect ratio 3:1 were produced by the acid-base method. Ensuing calcination altered particle size (slightly coarsening) and shape (nodular-like). Coatings obtained using calcinated powders produced through acid-base method were seen to be free of cracks before and after sintering.

 

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Presentation: Oral at E-MRS Fall Meeting 2006, Symposium A, by Onder Albayrak
See On-line Journal of E-MRS Fall Meeting 2006

Submitted: 2006-05-20 19:22
Revised:   2009-06-07 00:44