Search for content and authors
 

Detectors for EDE experiments.

Giuseppe Salvini 4Jon Headspith 4Stephen L. Thomas 3Gareth Derbyshire 3Andy Dent 4Trevor Rayment 5John Evans 2Richard Farrow 4Sofia Diaz-Moreno 1,3Cyril Ponchut 1

1. Europen Synchrotron Radiation Facility (ESRF), 6, Jules Horowitz, Grenoble 38000, France
2. University of Southampton, Department of Chemistry, Southampton SO17 1BJ, United Kingdom
3. Rutherford Appleton Laboratory (RAL), Chilton, Didcot, Oxon OX11 0QX, United Kingdom
4. Daresbury Laboratory (DL), Daresbury, Warrington WA4 4AD, United Kingdom
5. University of Cambridge, Department of Chemistry, Pembroke Street, Cambridge CB2 1TN, United Kingdom

Abstract

EXAFS, X-ray absorption spectroscopy fine structure, has been an important tool within synchrotron radiation science for some years. It has been used extensively in step scanning mode to provide information on the local environment within both static and slowly changing samples.
Energy dispersive EXAFS (EDE) allows similar information to be collected in a significantly shorter time frame, enabling the study of truly dynamically changing samples. The technique uses a bent crystal monochromator to focus an energy dispersed x-ray beam onto a sample which then impinges upon an array detector positioned behind the sample. This allows the absorption over a range of energies to be collected in a very short period. Until recently only few systems have existed for this technique, typically employing commercially available detectors originally constructed for other applications. These presented limitations in speed, energy resolution, linearity and dynamic range and could only follow changes in the millisecond range.
Using UK ESPRC grant funds, a new detector has been developed (XSTRIP) which shows great improvements over the above limitations. This has opened whole new areas of science to researchers.
This talk will present the technique, some of the historical limitations, the performance increase afforded by the XSTRIP system and an overview of the future direction of detectors for this most exciting and important technique.

 

Legal notice
  • Legal notice:
 

Presentation: invited oral at E-MRS Fall Meeting 2004, Symposium D, by Giuseppe Salvini
See On-line Journal of E-MRS Fall Meeting 2004

Submitted: 2004-05-12 19:59
Revised:   2009-06-08 12:55