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Effect of carbon interlayer on the protective properties of hydroxyapatite coating deposited on 316L stainless steel by sol-gel method

Bożena Pietrzyk 1Jakub Gawroński 1Tadeusz Błaszczyk 2

1. Technical University of Lodz, Institute of Materials Science and Engineering, 1/15 Stefanowskiego, Łódź 90-924, Poland
2. University of Łódź, Department of General and Inorganic Chemistry, Narutowicza 68, Łódź 90-136, Poland

Abstract

Hydroxyapatite (HAP) coatings were deposited on 316L stainless steel by the sol-gel method. The same technique was used also for deposition HAP coatings onto stainless steel substrates coated previously with carbon film by RF PACVD method. The HAP coatings were annealed in air at the temperature of 500oC and 700oC. Their morphology, chemical and crystalline structure were characterized using scanning electron microscopy , energy dispersive x-ray spectroscopy, Fourier transform infrared spectroscopy and X-ray diffraction. The protective properties of the coatings were investigated by means of electrochemical tests which were carried out in Tyrode’s solution.

It was found that both carbon and HAP coating improved corrosion resistance of stainless steel substrate. Protective properties of composite carbon-HAP coating depended on the temperature of heat treatment. The composite coating annealed at 500oC revealed better protective properties than that treated at 700oC.

 

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Related papers

Presentation: Poster at E-MRS Fall Meeting 2008, Symposium I, by Bożena Pietrzyk
See On-line Journal of E-MRS Fall Meeting 2008

Submitted: 2008-05-12 22:44
Revised:   2009-06-07 00:48