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iMATERIA - versatile neutron diffractometer at J-PARC

Toru Ishigaki 1Akinori Hoshikawa 1Masao Yonemura 2Kenji Iwase 1Dyah S. Adipranoto 1Tuerxun Wuernisha 1Takahiro Morishima 3Takashi Kamiyam 3Ryoko Oishi 3Kazuya Aizawa 4Masatoshi Arai 4Makoto Hayashi 5

1. Ibaraki University, Frontier Research Center for Applied Nuclear Sciences, 4-12-1 Nakanarisawa, Hitachi 316-8511, Japan
2. Ibaraki University, Institute of Applied Beam Science, 4-12-1 Nakanarisawa,, Hitachi 316-8511, Japan
3. High Energy Accelator Research Organization, Neutron Science Laboratory (KEK), 1-1 Oho, Tsukuba 305-0801, Japan
4. Japan Atomic Energy Agency, JPARC Center (JAEA), 2-4 Shirakatashirane, Tokai 319-1195, Japan
5. Ibaraki prefecture goverment (IBARAKI), 978-6 Kasahara, Mito 310-8555, Japan

Abstract

Ibaraki prefecture, the local government of the area for the J-PARC (Japan Proton Accelaror Research complex) site in Japan, decided to build a versatile neutron diffractometer (iMATERIA, IBARAKI Materials Design Diffractometer) to promote industrial applications of neutron beam research at J-PARC. iMATERIA was planned to be a high throughput diffractometer so that materials engineers and scientists can use this diffractometer like any other chemical analytical instrument in their materials development programs. It covers in d range 0.18 < d (Å) < 5 with Δd/d = 0.16 % for the high resolution bank, and covers 5 < d (Å) < 800 with gradually changing resolution at three detector banks (90 degree, low angle and small angle). Typical measuring time to obtain a ‘Rietveld-quality’ data set is several minutes with the sample size of a laboratory X-ray diffractometer. To promote industrial applications, we will establish a support system for both academic and industrial users who are willing to use neutrons but are not familiar with neutron diffraction. The analysis software is also very important for powder diffraction experiments, so we will also prepare a software package (Z-Code) consisting of a combination of several powder-diffraction software tools (Z-Rietveld, etc.), structural databases and visualization. The construction of iMATERIA was completed, as one of the day-one instruments for the J-PARC neutron facility.  Recent data of iMATERIA will be reported.

 

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Related papers

Presentation: Poster at 11th European Powder Diffraction Conference, Poster session, by Toru Ishigaki
See On-line Journal of 11th European Powder Diffraction Conference

Submitted: 2008-04-23 03:49
Revised:   2009-06-07 00:48