Plastic deformation is one of the methods of modifying the structure and properties of materials [1]. In conventional deformation techniques, the material loses its cohesion and undergoes destruction. Torsion applied under high pressure, known as the Bridgmen method, permits almost unlimitedly large deformation degrees [2]. The deformation process consists of torsion combined with compression. The iron samples have the shape of discs. The compressive pressure was about 5 GPa. After 5 rotations of the compressive punches, the maximum true strain obtained was e = 10. The structural inhomogeneity of the material thus deformed was examined. The microhardness was measured along 10 different radii (figure below). In the central point of the sample the microhardness was 268HV and it increases to about 470 HV towards the sample edges. The microhardness profiles are shown in the figure below. Optical microscopy shows characteristic concentric circles formed during the torsion. Electron microscopy has revealed uniaxial crystallites whose size ranges from 100 to 300nm. The dislocation density distribution is nonuniform both in the scale of the entire sample and in the microregions. [Image11.gif]
REFERENCES 1. V.M.Segal, Mat.Sc.Eng. A197 (1995), p.157; 2. F.Z.Utyashev, F.U.Enikeev, V.V.Latysh, Ann.Chim.Fr. 21 (1996), p.379.
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